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Home  ❯  Blog  ❯  Enhancing Bond Strength in Glass Fiber Composites With Plasma Cleaning

Enhancing Bond Strengthin Glass Fiber Composites with Plasma Cleaning

Enhancing Bond Strength in Glass Fiber Composites With Plasma Cleaning

  • Writen by Tina Jiao
  • December 13, 2024
  • Blog

Introduction

Plasma treatments have been used to improve the surface cleanliness and key properties of many materials. It can be particularly useful in various industries that rely on safety and perfect performance. Today, we will review the composition of glass fiber and how plasma cleaning can enhance its performance.

Understanding glass fiber composites

Glass fiber composites are high-performance materials made by embedding fibers within epoxy, polyester, or vinyl ester. These fibers serve as a reinforcement tool for the resin matrix that provides shape and additional tensile strength. The combination of materials boosts its mechanical properties while remaining extremely lightweight.

Glass fiber composites are strong and can withstand corrosion and extreme temperatures. They can handle heavy loads and function perfectly in harsher environments such as high altitudes for aerospace and marine industries.

 

Challenges in bonding glass fiber composites

Surface contamination

Surface contamination is the main challenge experienced when bonding glass fiber composites. Several contaminants, such as oil, dust, and other residues may prevent adhesives from adhering to the surface. This leads to weak bond formation and eventual failure of adhesion to coatings or other mechanical components.

Low surface energy

Glass fiber composites typically have low surface energy. This means that they do not react well with adhesives or coatings. This surface energy limits wettability and the bonding process, which means that adhesives do not form a strong chemical bond with the surface. As a result, the strength of the glass fiber composite will be significantly reduced.

Poor bonding

Glass fiber composites commonly experience increased separation of layers (delamination) due to weak adhesive bonding. These weak runs can compromise the structural integrity of the item and cause premature failure. This will significantly decrease safety and performance.

The role of plasma cleaning in enhancing bond strength

Plasma cleaning is a very useful tool that works by exposing the materials’s surface to ionized gas or plasma. This interacts with the surface and changes the molecular composition to improve bonding. 

Mechanisms of plasma cleaning

Plasma cleaning primarily removes surface contaminants, such as oil, dust, and other bacteria from the surface of the glass fibers. The treatment etches the glass fiber surface, which increases the surface energy. This allows the surface to better interlock with adhesives and other coatings. 

It uses hydroxyl, carbonyl, and amine groups to chemically increase surface energy. The plasma treatment alters the surface of the glass fiber composites to ensure the material is receptive to adhesive bonding.

By increasing the surface energy, coatings will spread better across the surface, leading to a reduction in imperfections. This enhanced wettability helps create strong bonds, which make the glass fiber composite more durable.

Impact on bond strength

A cleaner surface and increased surface energy will allow more reliable and stronger ones to form between the glass fiber composite surface and adhesives or coatings. Plasma cleaning promotes improved chemical interaction and better bond strength. This bonding potential is crucial in high-performance applications.

Benefits of plasma cleaning for glass fiber composites

Enhanced surface  cleanliness

The main benefit is the effective removal of surface contaminants. Traditional cleaning methods may not remove microscopic bacteria. However, plasma cleaning can thoroughly clean the surface on a molecular level. This will ensure the glass fiber composites have a clean surface for bonding with adhesives.

Increased surface energy

Plasma cleaning increases the surface energy of glass fiber composites by chemically etching the surface to increase wettability. This ensures that adhesives interlock better with the surface, which helps to create stronger bonding between the composite and the coating.

Improved durability and performance

Plasma-treated glass fiber composites often exhibit enhanced durability. The treatment process boosts the material’s ability to bond, which makes it more resistant to environmental factors such as increased moisture or humidity, extreme temperatures, and UV radiation. This ensures that the parts can remain strong/durable and perform better in these conditions over time.

Compatibility with various adhesives

Plasma cleaning can enhance the bonding potential with a variety of adhesives. This versatility makes plastic cleaning an attractive option for manufacturers who utilize different adhesive formulations depending on the type of glass fiber composite.

Applications of plasma cleaning in glass  fiber composite manufacturing

Aerospace industry

Plasma cleaning enhances the bonding strength of lightweight glass fiber composites, which are used to create aircraft wings, fuselage sections, and engine parts. Strong adhesive bonding is important to maintaining structural integrity and safety.

Automotive industry

Plasma cleaning is great at improving the bonding between vehicle parts, structural reinforcement, and crash-resistant panels in automobiles. The enhanced adhesion ensures better durability and vehicle performance.

Marine industry

In Marine environments, glass fiber composites are exposed to salt water, increased moisture, and UV radiation. These components are commonly used in boats and ships and must have strong and durable adhesive bondings to withstand these extreme conditions.

Sports equipment

Plasma-treated materials made from glass fiber composites are used in the production of sports equipment. These products such as bicycles, tennis rackets, golf clubs, etc. require increased strength to perform well during use. This means that the enhanced tensile strength of glass fiber composite materials needs to be reliably bonded to ensure safety.

Step-by-step process of plasma cleaning for glass fiber composites

Step-by-step process of plasma cleaning for glass fiber composites

Step 1 Preparation

Mechanical cleaning of the glass fiber composite parts is necessary to remove large particles or residue from initial production, which may impede the adhesion of future coating. At this stage, surface defects like cracks and scratches are identified, as they could worsen with treatment.

Step 2 Setup of equipment

This step entails prepping the vacuum chamber and plasma generator to ensure that all components are functioning before the process begins. Regulation of the gas flow and electricity needs to be inspected. Personal protective equipment and proper ventilation for the area must be coordinated. 

Step 3 Plasma treatment 

Once the parts are placed into the chamber and the parameters are set, including pressure duration and gas flow. The power generally ranges from 50 to 200 watts, at a pressure of 0.1 torr for 30 seconds to a few minutes.

Step 4 Post-treatment

At this stage, the machine is at rest until atmospheric pressure returns to normal, and then the parts are carefully removed to prevent recontamination. You can also conduct quality testing and other evaluations to confirm the effectiveness of the treatment process.

Evaluating the effectiveness of plasma cleaning

Several tests can identify the improvements in different properties of glass fiber composites. These methods are the shear test, lap shear test, peel test, and comparative analysis.

A shear test measures the force required to detach two bonded surfaces. Similarly, a lap shear test can assess the strength of adhesive bonds between two overlapping layers. These numbers can help indicate the increased strength of a bond between plasma-treated materials and non-plasma-treated materials.

A peel test can measure the force required to separate an adhesive layer from a composite surface. Due to the increased wettability and interlocking bonding of plasma treatments to glass fiber composites, it is important to identify the force necessary to break that bond over time.

Surface characterization

You can assess the changes in surface properties using contact angle measurements, surface roughness, and morphology. These tests can analyze surface energy improvements after plasma treatment.

A contact angle measurement test can assess the changes in surface energy and wettability. A surface roughness test can identify changes in surface topography at a nanoscale level. It will also indicate the mechanical interlocking strength of the plasma treatment surface. 

Surface morphology can visually identify the change in surface structure, which prevents contaminants from sticking to the surface while improving adhesion. It provides a detailed mapping of the microstructural changes.

Comparative analysis

A comparative analysis can provide evidence of improvements made by plasma cleaning to a surface. It can measure the durability, strength, wettability, and general performance over time.

Challenges and Considerations

A common challenge with plasma cleaning is the risk of overtreatment. Over-treatment occurs when the materials remain in the machine for longer than recommended. Over-treatment can damage the surface structure of the glass fiber composites and reduce strength and durability.

Another challenge that can be faced when considering plasma treatment is the cost of the equipment. The high implementation cost for the initial setup and continuous maintenance of the plasma treatment equipment. You need to consider the technological/ electrical energy and staff resources used during the process.

The cost of the equipment versus the long-term benefits that you will achieve from enhanced bonding strength and reduction in replacement costs. A cost-benefit analysis can assist in identifying the pros and the cons.

Another challenge one might face is the difficulty of customizing parameters during treatment. Treatment time and conditions will vary based on the specific glass fiber formulation and the adhesives that you may want to use. Tailoring these conditions will affect the effectiveness of the plasma treatment.

Conclusion

Plasma treatment can effectively remove contaminants and increase the surface energy of glass fiber composites. The process can ensure more durable adhesive bonds for industries such as aerospace, automotive, marine, and sports, where high-performance composite materials are essential.

With proper utilization of plasma treatment, you can increase the durability of items over time and experience better optimization for mechanical performance and longevity. If you are interested in purchasing your plasma cleaning equipment today, contact us for a free quote.

Author
Tina Jiao, Sales director of FARI, has 13+ years of experience in the plasma processor market in China. She is good at plasma treatment and plasma etching technology, and has served medium and large customers in many fields. If you have any questions, please feel free to contact.
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Fari was founded in 2011, is a professional manufacturing enterprise specializing in the research and development, production, sales and promotion of vacuum plasma cleaner and atmospheric plasma surface treatment technology equipment. 

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